Methyl chloroacetate → HCID 85706506, 화합물
반응식
[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[Cl:10])[CH:5]=[O:6].Cl[CH2:12][C:13]([O:15][CH3:16])=[O:14].C[O-].[Na+].CO>CO>[Cl:1][C:2]1[CH:3]=[C:4]([CH:5]2[O:6][CH:12]2[C:13]([O:15][CH3:16])=[O:14])[CH:7]=[CH:8][C:9]=1[Cl:10]참가 물질
5
실험 절차
To a solution of 3,4-dichlorobenzaldehyde (51.0 g) and methyl chloroacetate (51 mL) in methanol (500 mL) was added 28% sodium methoxide/methanol (68 mL) solution under ice-cooling, and the mixture was stirred at room temperature overnight. The resultant product was collected by filtration, and washed with distilled water to give the title compound (90.9 g).
후처리
- temperaturecooling
- filtrationThe resultant product was collected by filtration
- washwashed with distilled water
출처 및 근거
- ORD 기록
- ord-320308a3e3694e529aef9ab12a06f3f3
- 출처 데이터셋
- uspto-grants-2014_05
- 특허 번호
- US08722662B2
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