Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclopropanecarbonyl chloride → Ethyl 4-(cyclopropanecarbonyl)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclopropanecarbonyl chloride | HCID 77637 | — |
| 반응물 | HCID 178469116 | HCID 178469116 | — |
| 생성물 | Ethyl 4-(cyclopropanecarbonyl)benzoate | HCID 24724092 | — |
반응 단계
Intermediate i-3a was prepared from 4-ethoxycarbonylphenyl zinc iodide and cyclopropanecarbonyl chloride following the above procedure as described for intermediate i-1a. m/z (ES) 219 (MH)+. 1HNMR (500 MHz, CDCl3): δ 8.17 (d, 2H, J=8.5 Hz), 8.08 (d, 2H, J=8.4 Hz), 4.44 (q, 2H, J=7.1 Hz), 2.71 (m, 1H), 1.45 (t, 3H, J=7.1 Hz), 1.31 (m, 2H), 1.13 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08729104B2 |
| 출처 데이터셋 | uspto-grants-2014_05 |
| ORD ID | ord-7c88169332de4cee8e017c1347355d2a |
| 출처 메모 | uspto-grants-2014_05 |