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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1027349생성일: 2026년 10월 25일

Ethanol → Sodium 1,3,5-tricyclohexylbenzenesulfonate

https://huagongshe.com/reaction/1027349

반응식

참여 물질

역할이름HCID투입량
반응물EthanolHCID 702—
반응물Sodium HydroxideHCID 14798—
반응물Chlorosulfonic acidHCID 24638—
반응물TricyclohexylbenzeneHCID 3015433—
용매DichloromethaneHCID 6344—
생성물Sodium 1,3,5-tricyclohexylbenzenesulfonateHCID 86655172—

반응 조건

온도3 °C

반응 단계

30 g of tricyclohexylbenzene was dissolved in 50 ml of methylene chloride, and the solution was stirred under cooling at 3° C. Thereto, 15.2 g of chlorosulfonic acid was slowly added dropwise and after the dropwise addition, the reaction solution was stirred at room temperature for 5 hours. Subsequently, 10 g of ice was charged, and 40 g of an aqueous 50% sodium hydroxide solution was charged. Furthermore, 20 g of ethanol was added, and the mixture was stirred at 50° C. for 1 hour. Insoluble matters were removed by filtration, and the residue was distilled off under reduced pressure at 40° C. The precipitated crystals were collected by filtration and then washed with hexane to obtain 30 g of sodium 1,3,5-tricyclohexylbenzenesulfonate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08735048B2
출처 데이터셋uspto-grants-2014_05
ORD IDord-1ea40928f6ff43d2adaaf72d4e29f615
출처 메모uspto-grants-2014_05