Ethanethiol → HCID 178477307, 화합물

HRID 1027547노트

반응식

HRID 1027547 반응식
[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:18][CH2:19][N:14]([CH2:15][CH2:16]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH2:2]CCC.C(S)C>>[CH2:1]([S:6][C:7]1[C:8]([CH:12]2[CH:17]3[CH2:16][CH2:15][N:14]([CH2:19][CH2:18]3)[CH2:13]2)=[N:9][NH:10][CH:11]=1)[CH3:2]

참가 물질

3

반응물 2

HCID 6343EthanethiolHCID 178447695HCID 178447695, 화합물

생성물 1

HCID 178477307HCID 178477307, 화합물수율 30%

실험 절차

Compound 49D was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using ethanethiol as reagent. Subsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1) afforded compound 49D.

후처리

  1. customSubsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1)

출처 및 근거

ORD 기록
ord-72955bd6932947a594ed7350bf51dba4
출처 데이터셋
uspto-grants-2014_05
특허 번호
US08735388B2

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