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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1030740생성일: 2026년 10월 26일

1-[2-Hydroxy-4,6-bis(methoxymethoxy)phenyl]ethanone → 3,4-Bis(methoxymethoxy)benzaldehyde

https://huagongshe.com/reaction/1030740

반응식

참여 물질

역할이름HCID투입량
반응물1-[2-Hydroxy-4,6-bis(methoxymethoxy)phenyl]ethanoneHCID 10879697—
용매EthanolHCID 702—
생성물3,4-Bis(methoxymethoxy)benzaldehydeHCID 11746314218.6%

반응 단계

In 260 ml of ethanol were dissolved 33.37 g of the 2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone obtained in Production Example 11 and 32.20 g of the 3,4-bis(methoxymethoxy)benzaldehyde obtained in Production Example 24, and 300 ml of a saturated solution of potassium hydroxide in ethanol was added to the solution and the mixture was stirred for 24 hours to effect a reaction. After the reaction, the pH value of the reaction liquid was adjusted to about 6 by 6N hydrochloric acid, and the formed precipitate was recovered by filtration, washed with water and dried to obtain 53.17 g (yield=87.9%) of 2'-hydroxy-3,4,4',6'-tetrakis(methoxymethoxy)chalcone.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05106871
출처 데이터셋uspto-grants-1992_04
ORD IDord-ab4fe7a5970b4393aba04cc2d4a14e60
출처 메모uspto-grants-1992_04