Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 54338605, 화합물 → 1-[2,4-Bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 54338605 | HCID 54338605 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 1-[2,4-Bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone | HCID 19744892 | — |
반응 단계
Then, a suspension of 2.52 g of 5% palladium/carbon in 50 ml of ethyl acetate was hydrogenated for 2 hours, and a solution of 5.11 g of 2',4,4'-tris(methoxymethoxy)chalcone in 50 ml of ethyl acetate was added to the suspension and hydrogenation was carried out. After the reaction, the palladium/carbon was removed by filtration and the filtrate was concentrated under a reduced pressure to obtain 1-[2,4-bis(methoxymethoxy)phenyl]-3-(4-methoxymethoxyphenyl)-1-propanone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05106871 |
| 출처 데이터셋 | uspto-grants-1992_04 |
| ORD ID | ord-b83bb429686c41d5828f503d22c45b52 |
| 출처 메모 | uspto-grants-1992_04 |