Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 2-Acetyl-6-methoxynaphthalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1-(5-Bromo-6-methoxynaphthalen-2-yl)ethan-1-one | HCID 622178 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-Acetyl-6-methoxynaphthalene | HCID 77506 | — |
반응 단계
8.2 Grams of anhydrous aluminum chloride and 59 ml of toluene are added to the solution of 2-acetyl-5-bromo-6-methoxynaphthalene obtained in example 1, keeping the temperature at -10° C. The reaction mixture is kept under stirring at room temperature for 20 hours and then it is slowly poured into a mixture made by 200 g of crushed ice and by 75 ml of a 35% (w/v) aqueous solution of hydrochloric acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05107013 |
| 출처 데이터셋 | uspto-grants-1992_04 |
| ORD ID | ord-b0c0a35a8561482ba650ad8cca7fc128 |
| 출처 메모 | uspto-grants-1992_04 |