Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butanol → HCID 86745735, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butanol | HCID 6386 | — |
| 반응물 | Methyl Decanoate | HCID 8050 | — |
| 반응물 | (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal | HCID 107526 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 86745735 | HCID 86745735 | — |
반응 단계
25 ml of tertiary butanol was added to a mixture of 5.00 g (27.64 mM) of glucose and 1.03 g (5.55 mM) of methyl caprinate, and 100 mg of thermostable lipase derived from Candida antarctica (sp-382, manufactued by NOVO Co.) immobilized into an acrylic resin was further added. Then, they were refluxed under heating while stirring for 24 hours with an addition of 10 g of molecular sieves 5A as a methanol remover, to obtain glucose monocaprinate (C10 glucose ester).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05109127 |
| 출처 데이터셋 | uspto-grants-1992_04 |
| ORD ID | ord-344f50ca68b04784888a853a933057d8 |
| 출처 메모 | uspto-grants-1992_04 |