Benzyl Bromide → HCID 14155410, 화합물

반응식

[NH2:1][C:2]1[C:9]([Cl:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][OH:5].[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:5][CH2:4][C:3]1[CH:6]=[CH:7][CH:8]=[C:9]([Cl:10])[C:2]=1[NH2:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

반응물 2

HCID 7498Benzyl Bromide

HCID 14155407(2-Amino-3-chlorophenyl)methanol

생성물 1

HCID 14155410HCID 14155410, 화합물

실험 절차

This material was prepared from 2-amino-3-chlorobenzyl alcohol and benzyl bromide by the general procedure outlined in Example 98. The product was purified by Kugelrohr distillation to yield an oil, b.p. 118°-125° C. (0.1 mm). The product was characterized by IR and 1H NMR spectroscopy.

후처리

distillationThe product was purified by Kugelrohr distillation
customto yield an oil, b.p. 118°-125° C. (0.1 mm)

출처 및 근거

ORD 기록: ord-1f5814c9c3be4ddebd9d093bc9f7b711
출처 데이터셋: uspto-grants-1990_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04954163

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