Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1,1'-(Dithiodicarbonothioyl)bis(4-methylpiperazine)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 1-Methylpiperazine | HCID 53167 | — |
| 촉매 | Potassium ferricyanide | HCID 26250 | — |
| 생성물 | 1,1'-(Dithiodicarbonothioyl)bis(4-methylpiperazine) | HCID 30054 | — |
반응 단계
5 parts of N-methylpiperazine are reacted in 100 parts of water with 2 parts of sodium hydroxide and 4.2 parts of carbon disulfide and oxidized with 16.5 parts of potassium hexacyanoferrate(III). Obtained are 8.6 parts of the compound with 41.1% C, 6.5% H, and 15.7% N (calculated: 41.1% C, 6.3% H, 16.0% N, 36.6% S).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04956433 |
| 출처 데이터셋 | uspto-grants-1990_09 |
| ORD ID | ord-d62a17d3cd924e699fc26ff9dad7e5fb |
| 출처 메모 | uspto-grants-1990_09 |