Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(7-nitro-1H-indazol-4-yl)acetonitrile → 2-(3-Methoxy-4-nitrophenyl)acetonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(7-nitro-1H-indazol-4-yl)acetonitrile | HCID 13629308 | — |
| 반응물 | N,N-Dimethyl-N-[2-(3-methoxy-4-nitrophenyl)ethenyl]amine | HCID 54285175 | — |
| 생성물 | 2-(3-Methoxy-4-nitrophenyl)acetonitrile | HCID 13629317 | 99.3% |
반응 단계
19.8 g of N,N-dimethyl-N-[2-(3-methoxy-4nitrophenyl)ethenyl]amine and 30.0 g of hydroxylamineorthosulfonic acid are reacted as described in connection with preparing 2-(7-nitro-1H-indazol-4-yl)acetonitrile, thus obtaining 17.0 g of (3-methoxy-4-nitrophenyl)acetonitrile, mp 85°-86.5° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04958026 |
| 출처 데이터셋 | uspto-grants-1990_09 |
| ORD ID | ord-5e0df74fa9d84916b8697d0da74d71e9 |
| 출처 메모 | uspto-grants-1990_09 |