Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoic anhydride → Benzoic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoic anhydride | HCID 7167 | — |
| 반응물 | Acenaphthylene | HCID 9161 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Benzoic Acid | HCID 243 | — |
반응 단계
All reactions were run on a 10 mL scale at room temperature for a total of 5.00 min. The benzoic anhydride and internal standard were added from a stock solution which was 1.0M benzoic anhydride and 25,000 pm acenaphthylene in 100% acetonitrile. A total of 5.0 μL of this stock was used (yielding a 1:2000 dilution) to make each reaction 0.5 mM benzoic anhydride and 25 ppm acenaphthylene. Benzoic acid produced was measured by HPLC (high pressure liquid chromatography) using the acenaphthylene internal standard as a reference.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05308529 |
| 출처 데이터셋 | uspto-grants-1994_05 |
| ORD ID | ord-ff17610db45246418b847043e928669d |
| 출처 메모 | uspto-grants-1994_05 |