Diethylamine → HCID 4418042, 화합물

HRID 1033171노트

반응식

HRID 1033171 반응식
Cl[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][N:3]=1.[CH2:11]([NH:13][CH2:14][CH3:15])[CH3:12]>>[CH2:11]([N:13]([CH2:14][CH3:15])[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][N:3]=1)[CH3:12]

참가 물질

3

반응물 2

HCID 8021DiethylamineHCID 783082-Chloro-5-nitropyridine

생성물 1

HCID 4418042HCID 4418042, 화합물

실험 절차

Following Intermediate Method 5, the reaction of 2-chloro-5-nitropyridine, (XXII) with diethylamine produces 2-diethylamino-5-nitropyridine, (XXII). The reduction of this compound (XXII) with iron powder in aqueous hydrochloric acid and ethanol yields 5-amino-2-diethylaminopyridine, (XXIII).

출처 및 근거

ORD 기록
ord-93650fbb3a1b4ba5a55583b70df0acb0
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05310724

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