HCID 10241317, 화합물 → HCID 18651462, 화합물

HRID 1033410

반응식

HRID 1033410 반응식
[NH2:1][C@H:2]1[CH2:8][CH2:7][C:6]2[CH:9]=[CH:10][CH:11]=[CH:12][C:5]=2[NH:4][C:3]1=[O:13].[CH2:14]([O:21][C:22]([NH:24][C:25]([CH3:31])([CH3:30])[CH2:26][C:27](O)=[O:28])=[O:23])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH2:14]([O:21][C:22]([NH:24][C:25]([CH3:31])([CH3:30])[CH2:26][C:27]([NH:1][C@H:2]1[CH2:8][CH2:7][C:6]2[CH:9]=[CH:10][CH:11]=[CH:12][C:5]=2[NH:4][C:3]1=[O:13])=[O:28])=[O:23])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

3

반응물 2

HCID 10241317HCID 10241317, 화합물HCID 145510073-(((Benzyloxy)carbonyl)amino)-3-methylbutanoic acid

생성물 1

HCID 18651462HCID 18651462, 화합물

실험 절차

Prepared from 3(S)-amino-2,3,4,5-tetrahydro-1H-1-benzazepin-2-on (Example 1, Step B) and 3-benzyloxycarbonylamino-3-methylbutanoic acid (Example 1, Step E) by the procedure described in Example 1, Step F. FAB-MS: calculated for C23H27N3O4 409; found 410 (M+H,100%). [a]D =-160° (C=1,CHCl3).

출처 및 근거

ORD 기록
ord-c7452847358b4d96865ded3a4b4a74ac
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05310737

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