돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1033447생성일: 2026년 10월 26일

4'-(Bromomethyl)-2-cyanobiphenyl → 3-Benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1-[[2'-cyano-[1,1'-biphenyl]-4-yl]methyl]-1H-1-benzazepin-3-yl]-butanamide

https://huagongshe.com/reaction/1033447

반응식

참여 물질

역할이름HCID투입량
반응물4'-(Bromomethyl)-2-cyanobiphenylHCID 1501912—
반응물3-Benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1H-1-benzazepin-3-yl]-butanamideHCID 21836609—
생성물3-Benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1-[[2'-cyano-[1,1'-biphenyl]-4-yl]methyl]-1H-1-benzazepin-3-yl]-butanamideHCID 19025708—

반응 단계

Prepared from 3-benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1H-1-benzazepin-3-yl ]-butanamide (Example 51, Step A) and 4'-bromomethyl-1,1'-biphenyl-2-nitrile (Example 69, Step C) by the procedure described in Example 1, Step K. FAB-MS: calculated for C37H36N4O4 600; found; 601 (M+H,100%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05310737
출처 데이터셋uspto-grants-1994_05
ORD IDord-28c33a2d369b47b09497ffc31fdb2173
출처 메모uspto-grants-1994_05