HCID 14722828, 화합물 → HCID 22399592, 화합물

HRID 1033658노트

반응식

HRID 1033658 반응식
[CH:1]1([CH2:4][C:5]2[C:6]([OH:15])=[C:7]([CH:11]=[CH:12][C:13]=2[OH:14])[C:8]([NH2:10])=[O:9])[CH2:3][CH2:2]1.I[CH2:17][CH2:18][CH2:19][O:20][C:21]1[CH:34]=[CH:33][C:24]2[CH2:25][CH2:26][CH:27]([C:29]([O:31][CH3:32])=[O:30])[O:28][C:23]=2[C:22]=1[CH2:35][CH2:36][CH3:37]>>[NH2:10][C:8]([C:7]1[CH:11]=[CH:12][C:13]([O:14][CH2:17][CH2:18][CH2:19][O:20][C:21]2[CH:34]=[CH:33][C:24]3[CH:25]=[CH:26][CH:27]([C:29]([O:31][CH3:32])=[O:30])[O:28][C:23]=3[C:22]=2[CH2:35][CH2:36][CH3:37])=[C:5]([CH2:4][CH:1]2[CH2:3][CH2:2]2)[C:6]=1[OH:15])=[O:9]

참가 물질

3

반응물 2

HCID 14722828HCID 14722828, 화합물HCID 15341843HCID 15341843, 화합물

생성물 1

HCID 22399592HCID 22399592, 화합물

실험 절차

The compound of Example 66 and the compound of Example 23 are reacted together under the conditions described in Example 24. The crude product is purified by chromatography on silica gel using ethyl acetate/hexane (4:6) as eluant to afford the product.

후처리

  1. customThe crude product is purified by chromatography on silica gel
  2. customto afford the product

출처 및 근거

ORD 기록
ord-7eb969b88ebb49178a8446f4fbe2b04e
출처 데이터셋
uspto-grants-1994_05
특허 번호
US05310951

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