Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosgene → 1,2,3,4-Tetrahydroquinoline-1-carbonyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosgene | HCID 6371 | — |
| 반응물 | 1,2,3,4-Tetrahydroquinoline | HCID 69460 | — |
| 생성물 | 1,2,3,4-Tetrahydroquinoline-1-carbonyl chloride | HCID 13591069 | 90% |
반응 단계
By the procedure of Example 7, Step A, 1,2,3,4-tetrahydroquinoline was reacted with phosgene to give a 90% yield of the title compound as a dark orange oil, homogeneous by TLC (3:1 hexane-EtOAc) but Rf identical to that of starting material; IR spectrum νCO 1740 cm-1 ; FAB-MS m/e 196 (M+1)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05312820 |
| 출처 데이터셋 | uspto-grants-1994_05 |
| ORD ID | ord-e9f51f8f648a430da2349861bdac7755 |
| 출처 메모 | uspto-grants-1994_05 |