참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 3-(2-Methylpropenyl)benzonitrile | HCID 19024792 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Isobutylbenzonitrile | HCID 19024755 | 94% |
반응 단계
To a solution of 3-(2-methyl-1-propenyl)benzonitrile (5.80 g) in methanol (50 ml) was added 10% palladium on activated carbon (1 g), and the mixture was stirred under hydrogen atmosphere (3 atm) at 25° C. for 1 hour. The catalyst was filtered off and the liltrate was evaporated to give 3-isobutylbenzonitrile (5.52 g) as a pale yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05312829 |
|---|
| 출처 데이터셋 | uspto-grants-1994_05 |
|---|
| ORD ID | ord-f5fee2c5150e427682aeaa078f4e5058 |
|---|
| 출처 메모 | uspto-grants-1994_05 |
|---|
