2-Bromo-6-methoxynaphthalene → HCID 24829225, 화합물

HRID 1035602

반응식

HRID 1035602 반응식
Br[C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([O:12][CH3:13])[CH:8]=2)[CH:3]=1.[CH3:14][O:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1OB(O)O>>[CH3:13][O:12][C:7]1[CH:6]=[CH:5][C:4]2[C:9](=[CH:10][CH:11]=[C:2]([C:17]3[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=3[O:15][CH3:14])[CH:3]=2)[CH:8]=1

참가 물질

3

반응물 2

HCID 787862-Bromo-6-methoxynaphthaleneHCID 21940032(2-Methoxyphenyl)boric acid

생성물 1

HCID 24829225HCID 24829225, 화합물

실험 절차

The compound is prepared by the reaction of 2-bromo-6-methoxynaphthalene (300 mg, 1.26 mmol, 1 eq) with 2-methoxyphenylboric acid (192 mg, 1.26 mmol, 1 eq) according to method A within 18 h. Purification by column chromatography was not performed, but the raw product was used for further syntheses.

후처리

  1. customPurification by column chromatography

출처 및 근거

ORD 기록
ord-5706cd4bdc7b4f8c94aa47849be26287
출처 데이터셋
uspto-grants-2013_10
특허 번호
US08546392B2

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