Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boron tribromide → 6-(4-Hydroxyphenyl)-2-naphthol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boron tribromide | HCID 25134 | — |
| 반응물 | 2-Methoxy-6-(4-methoxyphenyl)naphthalene | HCID 11149734 | — |
| 생성물 | 6-(4-Hydroxyphenyl)-2-naphthol | HCID 11459006 | 98% |
반응 단계
The compound is prepared by reaction of 2-methoxy-6-(4-methoxyphenyl)-naphthalene (150 mg, 0.57 mmol, 1 eq) with boron tribromide (3.4 ml, 3.4 mmol, 3 eq) according to method G. Purification by column chromatography with hexane/ethyl acetate 9/1 as the eluent yields the desired product in a yield of 98%, 132 mg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08546392B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-115a30c013ea425488c9d55d705f1b01 |
| 출처 메모 | uspto-grants-2013_10 |