2,4-Dimethoxy-5-methylbenzaldehyde → HCID 67067645, 화합물

HRID 1037171

반응식

HRID 1037171 반응식
F[C:2]1[CH:3]=[CH:4][C:5](OC)=[C:6]([CH:8](O)[C:9]#CC2C=CC=CC=2)[CH:7]=1.[CH3:20][O:21][C:22]1[CH:29]=[C:28]([O:30][CH3:31])[C:27]([CH3:32])=[CH:26][C:23]=1[CH:24]=[O:25]>>[CH3:20][O:21][C:22]1[CH:29]=[C:28]([O:30][CH3:31])[C:27]([CH3:32])=[CH:26][C:23]=1[CH:24]([OH:25])[C:9]#[C:8][C:6]1[CH:7]=[CH:2][CH:3]=[CH:4][CH:5]=1

참가 물질

3

반응물 2

HCID 2516922,4-Dimethoxy-5-methylbenzaldehydeHCID 670676721-(5-Fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol

생성물 1

HCID 67067645HCID 67067645, 화합물수율 89%

실험 절차

Following the procedure used to prepare 1-(5-fluoro-2-methoxy-phenyl)-3-phenyl-prop-2-yn-1-ol, 2,4-dimethoxy-5-methyl-benzaldehyde (1.00 g, 5.55 mmol) was reacted to give the title compound (1.39 g, 89%). 1H NMR (400 MHz, DMSO-d6): δ 7.43-7.30 (m, 6H), 6.61 (s, 1H), 5.79-5.70 (m, 2H), 3.83 (s, 3H), 3.82 (s, 3H), 2.09 (s, 3H).

후처리

  1. customwas reacted

출처 및 근거

ORD 기록
ord-c8fcf08743344e19897de6e480a4a3d4
출처 데이터셋
uspto-grants-2013_10
특허 번호
US08546376B2

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