HCID 178521700, 화합물 → HCID 178507186, 화합물
반응식
C(OC(=O)[NH:10][C:11]1([C:14]2[NH:18][N:17]=[N:16][N:15]=2)[CH2:13][CH2:12]1)C1C=CC=CC=1>CO.[Pd]>[NH:15]1[C:14]([C:11]2([NH2:10])[CH2:13][CH2:12]2)=[N:18][N:17]=[N:16]1참가 물질
4
실험 절차
[1-(1H-tetrazol-5-yl)-cyclopropyl]-carbamic acid benzyl ester was dissolved in MeOH (5 ml). The solution was passed through a H-Cube hydrogenator at 0 bar, 30° C. and 1 ml/min with 10% Pd/C as a catalyst. The elute was concentrated to afford 48 mg of 1-(1H-tetrazol-5-yl)-cyclopropylamine as a solid product, m/z 126.5 [M+1]+.
후처리
- concentrationThe elute was concentrated
출처 및 근거
- ORD 기록
- ord-1a589d74c5f941b19ed54273a8c12adf
- 출처 데이터셋
- uspto-grants-2013_10
- 특허 번호
- US08552205B2
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