Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydrazinyl-4-iodopyridine → HCID 178453093, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydrazinyl-4-iodopyridine | HCID 53402897 | — |
| 반응물 | Tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate | HCID 86654345 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 178453093 | HCID 178453093 | — |
반응 단계
To tert-butyl (1-(2-formylquinolin-8-yl)piperidin-4-yl)methylcarbamate (112 mg, 0.303 mmol) in DCM (20 mL) was added 1-(4-iodopyridin-2-yl)hydrazine (78.4 mg, 0.333 mmol). The reaction mixture was stirred for 1 hour and then taken on to directly to the next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08557809B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-07166c0a1907496e8a191a1a6137e0bf |
| 출처 메모 | uspto-grants-2013_10 |