Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Boric Acid → Orthoboric acid, compound with 1,3,5-triazine-2,4,6-triamine (1:1)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | Melamine | HCID 7955 | — |
| 반응물 | Calcium Carbonate | HCID 10112 | — |
| 생성물 | Orthoboric acid, compound with 1,3,5-triazine-2,4,6-triamine (1:1) | HCID 10197992 | — |
반응 단계
First, 70 kg of orthoboric acid, 50 kg of melamine, and 1 kg of calcium carbonate were mixed by a Henschel mixer. Next, the mixture was placed in a constant temperature and humidity chamber at a temperature of 80° C. and a relative humidity of 80% for 2 hours to produce melamine borate. Then, the melamine borate was subjected to calcination and crystallization in a batch atmosphere furnace under a nitrogen atmosphere at 1750° C. for 2 hours to yield boron nitride with a graphitization index (GI) of 3.95 and a specific gravity of 2.27 g/cm3. After that, grinding was adjusted to prepare D-6 with a volume-average particle diameter of 18.0 μm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08557905B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-befd201c3ed0481bac2f6a7af77149bc |
| 출처 메모 | uspto-grants-2013_10 |