p-Toluenesulfonic acid → HCID 19703103, 화합물
반응식
[C:1]([O:4][N:5]=[C:6]([C:8]1[CH:13]=[CH:12][C:11]([I:14])=[CH:10][CH:9]=1)[NH2:7])(=O)[CH3:2].C1(C)C=CC(S(O)(=O)=O)=CC=1>C1(C)C=CC=CC=1>[I:14][C:11]1[CH:12]=[CH:13][C:8]([C:6]2[N:7]=[C:1]([CH3:2])[O:4][N:5]=2)=[CH:9][CH:10]=1참가 물질
4
실험 절차
To a solution of the product obtained in Step B above (9.7 g, 31.9 mmol) in 300 ml of toluene there are added 150 mg of para-toluenesulphonic acid and the reaction mixture is heated at reflux, using a Dean-Stark installation, for 24 hours. The mixture is evaporated to dryness and dried using a vacuum pump.
후처리
- temperaturethe reaction mixture is heated
- temperatureat reflux
- customThe mixture is evaporated to dryness
- customdried
출처 및 근거
- ORD 기록
- ord-1c06c3c2da6c4d7fbe4542b0c33f260c
- 출처 데이터셋
- uspto-grants-2013_10
- 특허 번호
- US08569285B2
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