Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1046018생성일: 2026년 10월 26일
Ethyl 2-cyano-3-ethoxy-2-butenoate → Ethyl 2-cyano-5-(dimethylamino)-3-ethoxypenta-2,4-dienoate
https://huagongshe.com/reaction/1046018
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethyl 2-cyano-3-ethoxy-2-butenoate | HCID 46635 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | Ethyl 2-cyano-5-(dimethylamino)-3-ethoxypenta-2,4-dienoate | HCID 54113151 | — |
반응 단계
A mixture of ethyl 2-cyano-3-ethoxybut-2-enoate (194 g theory, 1.06 mol) and N,N-dimethylformamide dimethyl acetal (160 g, 1.325 mol) was stirred at 70° C. for 2 hours. The mixture was concentrated under high vacuum to provide crude ethyl 2-cyano-5-(dimethylamino)-3-ethoxypenta-2,4-dienoate. The residue was used directly without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08569319B2 |
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| 출처 데이터셋 | uspto-grants-2013_10 |
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| ORD ID | ord-42b4674ae4bd4d4491db943b6f21a621 |
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| 출처 메모 | uspto-grants-2013_10 |
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