2-Fluoro-4-iodopyridine → Pyridine, 4-iodo-2-(methylthio)-

반응식

F[C:2]1[CH:7]=[C:6]([I:8])[CH:5]=[CH:4][N:3]=1.BrC1C=[C:14]([S:16]C)C=CN=1>>[I:8][C:6]1[CH:5]=[CH:4][N:3]=[C:2]([S:16][CH3:14])[CH:7]=1

참가 물질

반응물 2

HCID 70235702-Fluoro-4-iodopyridine

HCID 234370172-Bromo-4-(methylthio)pyridine

생성물 1

HCID 58485338Pyridine, 4-iodo-2-(methylthio)-

실험 절차

The title compound was prepared from 2-fluoro-4-iodo-pyridine following a procedure analogous to that described for 2-bromo-4-methylsulfanyl-pyridine in Example 184. Mass spectrum (ESI+): m/z=252 [M+H]+.

출처 및 근거

ORD 기록: ord-bc8f9128d81146b1a281f2775747612e
출처 데이터셋: uspto-grants-2013_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08569292B2

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