Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Azide → Diisobutyl aluminium azide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Azide | HCID 33557 | — |
| 반응물 | Diisobutyl aluminium chloride | HCID 16686353 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Diisobutyl aluminium azide | HCID 86610998 | — |
반응 단계
1.235 g of granular sodium azide (19 mmol) are added to a cold solution of diisobutyl aluminium chloride (19 mmol, 1.8M in toluene) diluted in 5 ml of toluene and the mixture is stirred at room temperature over the night to give diisobutyl aluminium azide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08569528B2 |
| 출처 데이터셋 | uspto-grants-2013_10 |
| ORD ID | ord-64e4130e48684bdfb9deb439bc89815c |
| 출처 메모 | uspto-grants-2013_10 |