참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Calcium chloride, dihydrate | HCID 6093260 | — |
| 반응물 | bicyclo2.2.1heptane-2,3-dicarboxylic acid, disodium salt | HCID 21981355 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Calcium bicyclo(2.2.1)heptane-2,3-dicarboxylate | HCID 21981350 | — |
반응 단계
To a solution of disodium bicyclo[2.2.1]heptane-2,3-dicarboxylate (22.6 g, 0.1 mol) in water (150 g) was added a solution of calcium chloride dihydrate (14.7 g, 0.1 mol) in water (100 g). The mixture stirred at 60° C. for 2 hours. The resulting white precipitate was filtered. The white powdery product was dried and milled (m.p. >300° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07094820B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_08 |
|---|
| ORD ID | ord-c0156d75e2c14a898911d22916c87e2d |
|---|
| 출처 메모 | uspto-grants-2006_08 |
|---|
