Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosphorus pentachloride → 1-Chloro-3-isocyanato-2-methylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosphorus pentachloride | HCID 24819 | — |
| 반응물 | HCID 5045840 | HCID 5045840 | — |
| 용매 | Chlorobenzene | HCID 7964 | — |
| 생성물 | 1-Chloro-3-isocyanato-2-methylbenzene | HCID 2735770 | — |
반응 단계
A mixture of the above-mentioned 1-chloro-2-methyl-3-methoxycarbonylaminobenzene 5.80 g, phosphorus pentachloride 7.53 g and chlorobenzene 50 mL was stirred with heating under reflux for one hour. The reaction mixtures were concentrated under reduced pressure to give 1-chloro-3-isocyanato-2-methylbenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09380782B2 |
| 출처 데이터셋 | uspto-grants-2016_07 |
| ORD ID | ord-c07e86bf39de478ca7a81d6dc5d44939 |
| 출처 메모 | uspto-grants-2016_07 |