HCID 23134613, 화합물 → 3-Ethoxy-2-methylaniline
반응식
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([N+:10]([O-])=O)[C:5]=1[CH3:13])[CH3:2]>[C].[Pd].C(O)C>[CH2:1]([O:3][C:4]1[C:5]([CH3:13])=[C:6]([CH:7]=[CH:8][CH:9]=1)[NH2:10])[CH3:2]참가 물질
4
실험 절차
A mixture of 1-ethoxy-2-methyl-3-nitrobenzene described in Reference Preparation example 2539.9 g, palladium-carbon (palladium 5%) 4 g and ethanol 200 mL was stirred at room temperature under hydrogen atmosphere for eighteen hours. The mixtures were filtered and the filtrates were concentrated to give 3-ethoxy-2-methylaniline 33.0 g.
후처리
- filtrationThe mixtures were filtered
- concentrationthe filtrates were concentrated
출처 및 근거
- ORD 기록
- ord-0124a7c0ff9a437f91fc0767421e3bb0
- 출처 데이터셋
- uspto-grants-2016_07
- 특허 번호
- US09380782B2
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