Hydrazine → HCID 4164367, 화합물
반응식
CS[C:3]([NH:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[C:4]([C:7]#[N:8])[C:5]#[N:6].[NH2:16][NH2:17]>CCO>[NH2:6][C:5]1[NH:17][N:16]=[C:3]([NH:9][C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:4]=1[C:7]#[N:8]참가 물질
4
실험 절차
A mixture of compound 6 (3.2258 g, 14.85 mmol) and hydrazine (742 mg, 23.16 mmol) in EtOH (20 mL) was refluxed for 30 min, at which time the reaction was complete as determined by TLC. The reaction mixture was poured into 100 mL ice water. The resulting precipitate was filtered and dried to give compound 7 (2.599 g, 88.1% yield, 99.8% purity) as a white powder.
후처리
- temperaturewas refluxed for 30 min, at which time the reaction
- filtrationThe resulting precipitate was filtered
- customdried
출처 및 근거
- ORD 기록
- ord-4d674f84d7bf4579b47f771c1c5eddeb
- 출처 데이터셋
- uspto-grants-2016_07
- 특허 번호
- US09382237B2
반응 노트
불러오는 중…