Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(2-methylphenyl)methanesulfonyl Chloride → N-[4-(2,4-Dioxo-1,2,3,4-tetrahydronaphtho[1,2-b][1,4]diazepin-5-yl)phenyl]-1-(2-methylphenyl)methanesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (2-methylphenyl)methanesulfonyl Chloride | HCID 2760661 | — |
| 반응물 | 5-(4-Aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione | HCID 117699167 | — |
| 생성물 | N-[4-(2,4-Dioxo-1,2,3,4-tetrahydronaphtho[1,2-b][1,4]diazepin-5-yl)phenyl]-1-(2-methylphenyl)methanesulfonamide | HCID 117699186 | 37% |
반응 단계
By using 5-(4-aminophenyl)-1H-naphtho[1,2-b][1,4]diazepine-2,4(3H,5H)-dione obtained in Example 1, (3), and o-tolyl-methanesulfonyl chloride, the title compound (yield 37%) was obtained in the same manner as that of Example 145.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09382236B2 |
| 출처 데이터셋 | uspto-grants-2016_07 |
| ORD ID | ord-c2e876baa7524b1ea6d127aa961fdbf4 |
| 출처 메모 | uspto-grants-2016_07 |