Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 4-chloro-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylate → Ethyl 4-[(5-methoxy-2-oxo-2,3-dihydro-1,3-benzothiazol-6-yl)amino]-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 4-chloro-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylate | HCID 21262606 | — |
| 반응물 | 6-amino-5-methoxy-1,3-benzothiazol-2(3H)-one | HCID 90014948 | — |
| 생성물 | Ethyl 4-[(5-methoxy-2-oxo-2,3-dihydro-1,3-benzothiazol-6-yl)amino]-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylate | HCID 73442308 | — |
반응 단계
75 mg (332 μmol) ethyl 4-chloro-7H-pyrrolo[2,3-d]pyrimidine-6-carboxylate (CAS-No: 187725-00-4) were transformed in analogy to example 1 using 6-amino-5-methoxy-1,3-benzothiazol-2(3H)-one to give after working up and purification 20.0 mg (15%) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09382255B2 |
| 출처 데이터셋 | uspto-grants-2016_07 |
| ORD ID | ord-63520f616092494cb8a169fe16399d56 |
| 출처 메모 | uspto-grants-2016_07 |