Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bromine → 4-Bromo-2,6-dinitroaniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bromine | HCID 24408 | — |
| 반응물 | 2,6-Dinitroaniline | HCID 69070 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 4-Bromo-2,6-dinitroaniline | HCID 3746608 | 86% |
반응 단계
A mixture comprising 247.5 g (1.35 mol) 2,6-dinitroaniline, 2.5 L acetic acid and 250 mL bromine was heated to 100° C. for a few minutes. After cooling, the formed crystals were filtered and washed with n-hexane to give 304 g (86%) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09388140B2 |
| 출처 데이터셋 | uspto-grants-2016_07 |
| ORD ID | ord-71fb586d4a5d439f89dfb3327ed607a9 |
| 출처 메모 | uspto-grants-2016_07 |