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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1055832생성일: 2026년 10월 26일

1-Isothiocyanato-2-(2-methoxyethoxyl)ethane → 8-iodo-3-(2-(2-methoxyethoxyl)ethyl)-2-(methyl-thio)quinazolin-4(3H)-one

https://huagongshe.com/reaction/1055832

반응식

참여 물질

역할이름HCID투입량
반응물1-Isothiocyanato-2-(2-methoxyethoxyl)ethaneHCID 22101683—
반응물8-iodo-3-(2-methoxyethyl)-2-(methylthio)quinazolin-4(3H)-oneHCID 89781985—
생성물8-iodo-3-(2-(2-methoxyethoxyl)ethyl)-2-(methyl-thio)quinazolin-4(3H)-oneHCID 89782139—

반응 단계

This compound (0.81 g, 1.92 mmol) was prepared according to the procedures described for Intermediate 715a, starting from 1-isothiocyanato-2-(2-methoxyethoxyl)ethane (716a; 0.67 g, 4.21 mmol). m/z (ESI, +ve ion) 421.0 (M+H)+.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US09394297B2
출처 데이터셋uspto-grants-2016_07
ORD IDord-11c5ccb481894f92b4984c0ad2ae4638
출처 메모uspto-grants-2016_07