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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 10570생성일: 2026년 10월 25일

Hydrochloride methanol → HCID 178418756, 화합물

https://huagongshe.com/reaction/10570

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloride methanolHCID 21893726—
반응물HCID 178418777HCID 178418777—
생성물HCID 178418756HCID 178418756—

반응 단계

According to the method of Example 1, Step C, deprotection was performed (room temperature, 2 hours) by using Intermediate 124 (83.9 mg) and 10% hydrogen chloride/methanol solution (2 ml). The solvent was evaporated under reduced pressure, and the residue was added with methanol (0.5 ml) and diethyl ether (1.5 ml). The deposited precipitates were collected by filtration and washed with diethyl ether to obtain the title compound (63.3 mg).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07094789B2
출처 데이터셋uspto-grants-2006_08
ORD IDord-98d12fb782ec41e3aba8ea2af660275d
출처 메모uspto-grants-2006_08