Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 178418777, 화합물 → HCID 178418696, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 178418777 | HCID 178418777 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | HCID 178418696 | HCID 178418696 | 45.2% |
반응 단계
A solution of Intermediate 124 (90.5 mg) in methanol (5 ml) was added with platinum oxide (13 mg, Wako Pure Chemical Industries) and stirred for 15 hours under hydrogen atmosphere. The reaction mixture was filtered through a Celite layer, and the solvent was evaporated under reduced pressure. Then, the residue was purified by silica gel column chromatography (chloroform:methanol=20:1) to obtain the title compound (41.1 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094789B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-41aab4904af540338d435ca329ed8c84 |
| 출처 메모 | uspto-grants-2006_08 |