N1,N1-Dibenzylethane-1,2-diamine → Benzathine

HRID 1057393

반응식

HRID 1057393 반응식
C([N:8]([CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH2:9][CH2:10][NH2:11])C1C=CC=CC=1>O>[CH:16]1[CH:17]=[CH:18][C:13]([CH2:12][NH:11][CH2:10][CH2:9][NH:8][CH2:12][C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)=[CH:14][CH:15]=1

참가 물질

3

반응물 1

HCID 6394114N1,N1-Dibenzylethane-1,2-diamine

생성물 1

HCID 8793Benzathine

시약·촉매·용매 1

HCID 962Water용매

실험 절차

HPLC analysis shows there to be 19.7% N,N dibenzylethylenediamine and 80% compound of Example 42 to be present by total area analysis. Water is present at 0.3%. This gives a stoichiometric ratio of compound to base of 1:0:5.

후처리

  1. customThis gives a stoichiometric ratio of compound to base of 1:0:5

출처 및 근거

ORD 기록
ord-dd6d9e155ecc4ebfb89127bc8f8219c4
출처 데이터셋
uspto-grants-2003_02
특허 번호
US06514975B1

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