Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxycatechol → 4-Methoxy-spiro[1,3-benzodioxole-2,1'-cycloheptane]
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxycatechol | HCID 13622 | — |
| 반응물 | 1,1-Dimethoxycycloheptane | HCID 12892877 | — |
| 생성물 | 4-Methoxy-spiro[1,3-benzodioxole-2,1'-cycloheptane] | HCID 22734096 | — |
반응 단계
Substantially the same procedure as in Reference Example 63 was repeated using 3-methoxycatechol (18 g) and dimethoxycycloheptane (24.35 g) to give Compound IIbm-a (28.0 g, 93.5%) as a colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06514996B2 |
| 출처 데이터셋 | uspto-grants-2003_02 |
| ORD ID | ord-fe8006f3cf9c460a8aff2b7bee78aebf |
| 출처 메모 | uspto-grants-2003_02 |