Benzyl chloroformate → HCID 178465414, 화합물

반응식

[NH2:1][CH:2]([PH:4](=[O:6])[OH:5])[CH3:3].Cl[C:8]([O:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[O:9]>>[C:12]1([CH2:11][O:10][C:8]([NH:1][CH:2]([PH:4](=[O:5])[OH:6])[CH3:3])=[O:9])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

참가 물질

반응물 2

HCID 10387Benzyl chloroformate

HCID 3018298Aminoethylphosphinic acid

생성물 1

HCID 178465414HCID 178465414, 화합물

실험 절차

The process is performed according to the operating conditions described in 1.4., starting with 1.7 g (15.6 mmol) of (1-aminoethyl)phosphinic acid and 3.12 g (18.29 mmol) of benzyl chloroformate. 2.8 g of product are recovered (yeld=73.9%).

후처리

custom2.8 g of product are recovered (yeld=73.9%)

출처 및 근거

ORD 기록: ord-d591f6ba6a6c43e6a4e593f2c2df6e51
출처 데이터셋: uspto-grants-2003_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06518260B1

반응 노트

불러오는 중…