Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-butyl N-{[4-(aminomethyl)phenyl]methyl}carbamate → N-(tert-butoxycarbonyl)-N'-[(5-isoquinolyl)sulfonyl]-1,4-xylylenediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-butyl N-{[4-(aminomethyl)phenyl]methyl}carbamate | HCID 3354775 | — |
| 반응물 | Isoquinoline-5-sulfonyl chloride hydrochloride | HCID 13116932 | — |
| 생성물 | N-(tert-butoxycarbonyl)-N'-[(5-isoquinolyl)sulfonyl]-1,4-xylylenediamine | HCID 69523966 | 82.7% |
반응 단계
According to Reference Example 5, Step B, a reaction was performed by using isoquinoline-5-sulfonyl chloride hydrochloride (10 g) and Intermediate 59 (8.96 g) to obtain the title compound (13.39 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094789B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-cc24d669fdfd47959b83d7a2b71561b6 |
| 출처 메모 | uspto-grants-2006_08 |