Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pyridine → 2-(2',6'-Diisopropylphenylazo)-4,6-ditertbutylphenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | 2,4-Di-tert-butylphenol | HCID 7311 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Diisopropylaniline | HCID 32484 | — |
| 반응물 | Phenolate | HCID 119047 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-(2',6'-Diisopropylphenylazo)-4,6-ditertbutylphenol | HCID 135723497 | — |
반응 단계
This phenol was prepared, as described for above, from a theoretical yield of 7.4 mmol of diazotized 2,6-diisopropylaniline and a phenolate solution comprised of 2,4-Ditertbutylphenol (1.42 g), water (15 mL), NaOH (0.5 g), pyridine (3 mL), and toluene (6 mL) Yield=0.98 g (36%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07094848B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-327e3218e975482ebbe892dcbab483af |
| 출처 메모 | uspto-grants-2006_08 |