Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Ethoxy-4-nitrobenzoic acid → 4-Amino-3-ethoxybenzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Ethoxy-4-nitrobenzoic acid | HCID 22397509 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 4-Amino-3-ethoxybenzoic acid | HCID 22397448 | 92.1% |
반응 단계
3-Ethoxy-4-nitrobenzoic acid (0.31 g) was treated with 5% palladium on charcoal under an atmosphere of hydrogen (1 bar) for 3 hours. The reaction mixture was filtered and the filtrate was evaporated to leave the product as a beige solid (0.245 g; MS: ES− (M-H) 180).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06525070B2 |
| 출처 데이터셋 | uspto-grants-2003_02 |
| ORD ID | ord-6030d1e15c2643c79bc1c31082b9bb2a |
| 출처 메모 | uspto-grants-2003_02 |