6-cyanobenzofuran-2-carboxylic Acid → HCID 22709960, 화합물

반응식

[C:1]([C:3]1[CH:14]=[CH:13][C:6]2[CH:7]=[C:8]([C:10]([OH:12])=O)[O:9][C:5]=2[CH:4]=1)#[N:2].Cl.[Cl:16][C:17]1[CH:18]=[C:19]2[C:24](=[CH:25][CH:26]=1)[CH:23]=[C:22]([S:27]([N:30]1[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]1)(=[O:29])=[O:28])[CH:21]=[CH:20]2>>[Cl:16][C:17]1[CH:18]=[C:19]2[C:24](=[CH:25][CH:26]=1)[CH:23]=[C:22]([S:27]([N:30]1[CH2:31][CH2:32][N:33]([C:10]([C:8]3[O:9][C:5]4[CH:4]=[C:3]([C:1]#[N:2])[CH:14]=[CH:13][C:6]=4[CH:7]=3)=[O:12])[CH2:34][CH2:35]1)(=[O:28])=[O:29])[CH:21]=[CH:20]2

참가 물질

반응물 2

HCID 107739206-cyanobenzofuran-2-carboxylic Acid

HCID 227097661-(6-Chloronaphth-2-ylsulphonyl)piperazine hydrochloride

생성물 1

HCID 22709960HCID 22709960, 화합물

실험 절차

In a similar manner to Referential Example 12 except for the use of 6-cyanobenzofuran-2-carboxylic acid and 1-[(6-chloronaphthalen-2-yl)sulfonyl]piperazine hydrochloride as the raw materials, the reaction was conducted, whereby the title compound was obtained.

출처 및 근거

ORD 기록: ord-f84dc96d767b4330958fe377a3c2ec0b
출처 데이터셋: uspto-grants-2003_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06525042B1

반응 노트

불러오는 중…