참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | N-Benzoyl-DL-phenylalanine | HCID 273362 | — |
| 생성물 | 4-Benzyl-2-phenyl-2-oxazolin-5-one | HCID 2756650 | 85.5% |
반응 단계
A suspension of N-benzoyl-DL-phenylalanine (5.39 g) and acetic anhydride (12.3 g) is stirred at 80° C. for 40 minutes under a nitrogen atmosphere. The reaction mixture is concentrated under reduced pressure to give the titled reference compound (4.30 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06960575B2 |
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| 출처 데이터셋 | uspto-grants-2005_11 |
|---|
| ORD ID | ord-92de09d394204087a6759572d4dc5add |
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| 출처 메모 | uspto-grants-2005_11 |
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