Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4-(Methanesulfonyl)benzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | p-(Methylsulphonyl)benzoic acid | HCID 77670 | — |
| 생성물 | 4-(Methanesulfonyl)benzoyl chloride | HCID 11276013 | — |
반응 단계
A mixture of 11.2 g (0.056 mol) of p-methylsulfonyl-benzoic acid prepared in Example 4 and 30 ml of thionyl chloride were heated under reflux to give a clear solution. Removal of the excess of thionyl chloride under reduced pressure obtained white solid and without purification put into the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06960611B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-dc2391ad1b0d413495c6bf541d6f4f16 |
| 출처 메모 | uspto-grants-2005_11 |