Benzoic Acid → 2-Amino-5-methylbenzophenone

HRID 1061865노트

반응식

HRID 1061865 반응식
[C:1]([OH:9])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:10][C:11]1[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=1>>[NH2:10][C:11]1[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][C:12]=1[C:1]([C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)=[O:9]

참가 물질

3

반응물 2

HCID 243Benzoic AcidHCID 7813p-Toluidine

생성물 1

HCID 873352-Amino-5-methylbenzophenone수율 49.3%

실험 절차

The procedure was in the same manner as described in example 15, except that the starting material was benzoic acid instead of p-chlorobenzoic acid and p-toluidine instead of 4-chloroaniline. The title compound was obtained as yellow needle crystal, and yield 49.3%, m.p. 64-66° C.

출처 및 근거

ORD 기록
ord-ec813877d1e64c6791fb325c41b30e17
출처 데이터셋
uspto-grants-2005_11
특허 번호
US06960611B2

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