Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenylboronic Acid → N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenylboronic Acid | HCID 66827 | — |
| 반응물 | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| 생성물 | N-(3-Nitro[1,1'-biphenyl]-4-yl)carbamic Acid tert-Butyl Ester | HCID 57745588 | 93.2% |
반응 단계
Prepared from (4-iodo-2-nitro-phenyl)-carbamic acid tert.-butyl ester (Example A1) (994 mg, 2.73 mmol) and phenyl boronic acid (576 mg, 3.00 mmol) according to the general procedure B. Obtained as a bright yellow solid (800 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06960578B2 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-2964a1ec3e414c80bc5c23ab787de4f0 |
| 출처 메모 | uspto-grants-2005_11 |