Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3-Ethylbenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Benzoic acid, 3-ethyl- | HCID 96207 | — |
| 촉매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Ethylbenzoyl chloride | HCID 12809323 | — |
반응 단계
3-Ethylbenzoic acid (9.40 g, 62.6 mmol) was added slowly to thionyl chloride (45 mL) at 0° C., and N,N-dimethylformamide (3 drops) was added dropwise. The obtained reaction mixture was refluxed under heating as it was for 2 h. The reaction mixture was concentrated and used without purification in the next reaction.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06962933B1 |
| 출처 데이터셋 | uspto-grants-2005_11 |
| ORD ID | ord-d2a2341ea8204d60af313ec6cefd3139 |
| 출처 메모 | uspto-grants-2005_11 |